American Underworld – Steroids – UGL! See what you injecting!!!!! stop to inject UGL NOW!

Basics oil-based parenterals.
Analyses – manufacturing and kitchenchemistry made .
Well, everybody knows that steroid based injections are faked. We will pass by the meter why it happens and will discuss how it happens and what could we do
to avoid fakes. First of I would like to show you how the oil-based parentals are normally made. After that I’ll try to discover basics of quality testing and some advanced things in brief.

So, lets discus the simplified technical process.
For the manufacturing required “vehicle” solution which is contains pharmaceutical parental-grade oil with excipients which are suppress bacteria
growth and enhances solubility of the API i.e. steroid ester as well as could suppress oxidation of the API. Normally, excipients such as benzyl alcohol are
reducing the pain in site of injection, but this is not in the case of fake. I would say faker’s formulation induces pain in the site of injection (I’ll explain later why). The theory of the preparation of the oil-based formulation is simple. Oil-based vehicle controls water content i.e. blood and lymph access at the injection site to make a long term effect. Excipients like benzyl alcohol (BA) are typically added in amount of 9 mg/ml of formulation, this level is considered to be optimal for the local anesthesia. Fakers some times use BA as a solubility enhancer in order to have better solubility of low-quality API.
The concentration of BA could reach 5% in such formulations. In such dozes BA acts as a cytotoxic agent which is induces local necrosis in the injection site. This is not very dangerous but extremely unpleasant. Being injected not deep (for example 10-15 mm in depth) such formulation causes necrosis between muscle and skin, this can cause serious discomfort and could be dangerous because injection site is continue bleeding thus could be infected. What else? I think that fake formulations do never content anti-oxidation agents. Factory made formulations could contain antioxidant or argon (noble gas) above the liquid. Usually, fakers unable to fill vials with argon during corking.

Now lets discuss oil and API. These two components are added in a significant amount to the formulation, so the quality of them is not unimportant. Oils are
widely used in different applications so there are many quality grades of them. Usually oils for pharmaceutical applications are good enough and not hazardous,
but being improperly stored or operated oil could be polluted with moisture, bacteria and sediments. Usage of non-pharmaceutical oils, thanks god, is rear.
API is produced in different grades as well. There are several grades of quality human-grade for parenterals or for tabs, GMP-grade, animal grade. Some good
guys are telling “we use human grade API for the dog formulations” some bad ones telling “we use animal grade stuff on humans”. All of them are not very
hazardous if operated and stored properly. Typically, the main problem of API
is the content of free hormone, i.e. testosterone enanthate contains more or less free testosterone and some amount of enantic acid. These components are
not hazardous, but significant content of the testosterone causes low temperature sedimentation of the drug or turbidity. Fakers are trying to suppress this effect by overdosing BA. Widespread problem is the presence of moisture in formulation. This is a key feature that allows verify the quality of a drug. Where is the moisture coming from? First of, low quality oil, API stored in refrigerator in an opened can (fakers are usually makes small amounts, so they can not use factory pack at once), and the third path-way ¬ through bad stoppers during the sterilization in water-steam autoclave. In general, moister is the enemy number one of oil-based formulations, especially if it is a handicraft drug. Moisture causes hydrolysis of ester, loss of solubility, turbidity and sedimentation of the API. How we do detect moisture?
We can look if the oil in vial is wetting the glass. Low quality mixtures have a poor wetting. We can check if the sediments are present as well. It is easy ¬
take a laser pointer, shake vial vigorously and watch for the particles in passing light, use a dark room to find illuminated particles. Sediments are coming to handicraft with oil, API powder, and from ambient air (it could be just a usual dust). Factory made drugs are produced in dust-free rooms, API and oil are stored in sealed cans. Before the packing oil solution is normally filtered through 0,22 mkm filter. It is obviously that factory-made drugs have no sediments.

I discovered basics methods of a fake detection and some ideas where problems are come from and how to find them fast, – the pain in the injection site, moisture detection and sediments detection. These methods are not very reliable. Sure, if you will find the turbidity or sediments it is 99% fake. But sometimes you will be unable to check the drug with these methods. Now I’ll describe I brief advanced techniques and methods of chemical analysis. In general there are two major problems here ¬ the dosage and the API kind. It is well-known problem when API is under dosed and if it is substituted with another one, or the both cases in the same time ¬ for example vial contains 25 mg/ml of trenbolone acetate and 25 mg/ml of testosterone propionate instead of 50 mg/ml of trenbolone acetate. Here is two kinds of techniques are employed ¬ quantitative analysis to determine API content and qualitative analysis to determine the nature of API added.

Quantification.
This type of analysis could be made according USP recommendations. There are different methods may be employed ¬ high-performance liquid chromatography
(HPLC) and spectrophotometry in ultra-violet range(UV). Both of methods have disadvantages, so the analysis should be made by qualified specialists.

HPLC.
This method is based on the separation of the drug formulation to individual compounds and quantitative analysis of the target compounds buy UV-detector.
For the separation the solution of drug in isopropyl alcohol is injected to a chromatographic column. Different compounds have a different linear migration speed in this column, so they are separated according the specific retention which is considered to be individual to each compound. Normally, long chain esters are not perfectly separated by conventional commercial HPLC instruments. Adaptation of the instrument for the silica gel column is expensive and usually analysis are made in low-cost way using conventional reversed-phase columns C8 or C18. Thus compounds are moving with different speed we can identify a target ester using migration time. Quantification in HPLC is provided by a UV spectrophotometric detector. USP recommends wavelength 240 nm for the quantification of testosterone esters and nandrolone esters, many others could be detected at same wavelength as well. This wavelength corresponds to the maximum of UV light absorption by steroids. Short wavelengths are not recommended due to non-specific absorption.

It is believed that HPLC coupled to diode array detector could provide the identification of steroid base. I think that it is not reliable technique, most of steroid bases have similar structure, so they will have a similar UV spectra. Sure, some steroids as trenbolone have unique fingerprint in UV but many others are too similar.

To find a concentration of ester we can add an additional known amount of pure ester. To have a good quantification more then 2 additives are necessary, i.e. if we have a concentration about 50 mg/ml of testosterone propionate we need to analyse this sample we should make a picture of this sample and two pictures
with standard additives to the sample solution of testosterone propionate. For the testosterone mixtures such sustanon concentrations of esters could be recalculated to molar concentrations in order to make quantification using single ester as a standard.

UV-Vis spectrophotometry.
This method is well known low-cost way to determine the content of many different compounds by the specific light absorption. This method employees a
simple principle ¬ the light absorption is proportional to the compound concentration. For all chemical compounds there is a wavelength where compound
absorbs the light. For most steroids the best wavelength is 240 nm. But it is virtually impossible to measure concentration of testosterone ester in this region in a drug. This problem caused by benzyl alcohol which is have a strong absorption at 240 nm. Benzylbenzoate has a similar high absorption (by weight).
It is possible to reduce concentration of BA by chemical manipulation, but if formulation contains BB, UV-Vis gives up.

Of the content of the two ampoules Aburaihan® a chemical analysis was performed through means of spectrophotometry The spectra of the photometry stand below just as the reference spectrum of testosterone. Where you should look for is the number under the peak of the line in the spectrum (note: the horizontal scale is not totally equal in both spectra).

The spectrum of the reference testosterone. The peak lies at 241nm!

The spectrum of the counterfeited vial. The peak lies here also at 241nm! This means it contains real testosterone

The spectrum of the fake ampoule. The horizontal scale is something larger here. The peak lies here by 272nm! This means it contains no testosterone. For the making of the both spectra, the real solution has
been diluted much further then the fake solution. If the spectra would have been made at the same concentration, then the peak in the fake spectrum much lower be. Again an indication that it for this
reason a whole other matter goes and also a good indication that it for this reason possible not an androgenic steroid goes. If last yet a thin low chromatogram.

Thin-layer Chromatography
All hormones have a different solubility in a given solvent (mostly methanol). These solubility differences are used to separate and identify the steroids on a thin layer plate. This plate consists of a thin layer of porous material that is coated on one side of a plastic, glass, or aluminium plate. The (diluted) solutions of steroids are applied on different spots of the plate, wich is then placed in a developing chamber containing a solvent bath.
As the solvent creeps up the plate by capillary action, it will wash the steroids of their original spots and carry them upwards towards the other end of the plate, some will have to migrate farther from the origin than the others. Thus this chromatographical pattern may be used to identify characteristics of the steroids. The plate can be studied in an ultraviolet viewing box. On the plate also a reference substance is placed, wich can be bought at several different pharmaceutical companies like by example Sigma or Fluka.
The thin-layer chromatography has a few minor disadvantages . Some compounds like by example Testosterone and Boldenone can’t be separated.

Where you to must look is or it well or not a spot sit in a straight line above the numbers at the bottom the plate. (R = reference pure testosterone, 1 = real Aburaihan, 2 = first tested nepvial, 3 = second
tested nepvial). What clear to see is, is that there in the nepvials no detecteerbare dust stretch. It stretch namely no dark spot on the plate what uses is for the separation. Also there a difference in the height of the spot for the pure
testosteron and the enanthaat is. This is precise as it hears! The exact theories explain goes here too far, but the spot for the enanthate sit where he must sit. Conclusion: in the nepvials, no testosterone enanthate or a comparable steroid
sit. In the real vial, testosterone enanthate sit.

Explanation of the picture Dilution 100* in methanol. Measured at 254nm on Merck TLC plates with fluorescentic layer. From the real Aburaihan® I yielded 1 micro litre on the plate from the fake 2 micro litres is yielded. This has been done to see the benzyl alcohol. This is unfortunately not visible on the picture t, but with the naked eye one sees is a very vague spot, where the benzyl alcohol sat on the TLC. It is possible to make the benzyl alcohol visibly, by adding more of the solution onto the plate.

API identification.
There are few methods which are allows to get a fingerprint of the molecular structure. These methods are widely used in chemical analysis, molecular structure research and have a forensic grade reliability due to detailed fingerprint of all molecular parts or atoms. These methods are:

1. Infrared spectra, or Fourier ¬ transform infrared, FTIR. The most suitable for oil formulations technique is FTIR identification, this method allows direct measurement of spectra in the oil solution. FTIR spectrometer coupled to multiple internal reflectance (MIR) accessory allow both ¬ fingerprint and quantification of the drug. There is the broad number of manufactures of such equipment: PerkinElmer, Bruker, Thermo-Nicolet, Varian, Shimadzu and many others.
2. Electron-impact mass-spectra ¬ EI/MS, usually coupled to gas chromatography. This method is widely used and named GC-MS. These equipment is widely used, but not the best for this kind of analysis, manufactures are: Thermo, Agilent, PerkinElmer, Shimadzu, Varian and many others.
3. Nuclear magnetic resonance spectra, NMR, of two kinds ¬ proton magnetic resonance (PMR) and C13 isotope magnetic resonance spectra, C13-NMR. This
equipment is expensive and made by Bruker, Hitachi, Varian, Shimadzu.
4. Liquid chromatography coupled to mass-spectrometer. Well, usual LC-MS just do not gives structural information. This technique shows only molecular weight
1. Instruments used for the molecular fingerprinting are terribly expensive because of presence of 2 or 3 or even 4 mass analyzers in the instrument. LC units made by: Waters, Agilent, PerkinElmer, Varian, Shimadzu. MS units made by: Bruker, ABI-Sciex.
5. Melting

Wet chemistry.
Instrument ¬ based analysis have there limitations. Concerning oil solutions of long-chain esters these disadvantages are critical. Only FTIR/MIR allow identify ester directly with minimum sample manipulation. Other techniques require sample preparation or even preparation of pure steroid base. At this point professional analysts starts there game. Typical pathways has there target in obtaining of pure steroid ester or steroid base or reducing of interfering effects of benzyl compounds. There are several basic techniques ¬ the freezing of oil at low temperature with different additives to cause the precipitation of ester, vacuum evaporation of benzyl alcohol, hydrolysis of a sample in order to have a steroid base. These techniques could be employed one-by-one to have a desired effect.

The July 2011 issue of FLEX Magazine features 2008 Mr. Olympia Dexter Jackson in, “You CAN Teach an Old Dawg New Tricks.” The article focuses on four unique exercises Jackson and Charles Glass (his trainer) implemented in Jackson’s preparation for the 2011 FLEX Pro. Each move has a specific focus and required precise technique! Now you can see and hear how to do each of the moves right from “The Blade” himself. Check out the video below and pick up the July 2011 issue of FLEX to see more!

HERE IS VIDEO TO SEE !!!!

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Read this before you use UG (UNDERGROUND STEROIDS) products!! by w_llewellyn

I just want to make a very clear statement as to my position on the use of Underground Steroids. This forum is public and uncensored barring our rules for dealing drugs and improper behavior. There is often a lot of discussion about this or that underground lab. How excellent the products are, and how they are perfectly pure etc. etc. I want to make sure everyone reading understands what underground steroids really are.

Underground labs are illegal unlicensed operations. It is not possible for these labs to directly purchase bulk pharmaceutical quality steroids to package for the public. Very few, if any, have the resources to obtain true USP (99+% tested pure) materials. Fewer still would spend the money on these materials even if they could obtain them, as they are very expensive.

Instead, underground labs obtain their drugs (99%) from unlicensed Chinese brokers. The thing you need to understand about China is that it has a strong regulated drug market. The U.S. buys a lot of real drugs from China. HOWEVER – The steroids we are talking about are very very rarely produced at pharmaceutical facilities.

The VAST MAJORITY of bulk steroids coming from China are produced in chemical companies. Imagine if you will a company that makes pesticides, synthetic dyes, or other manufacturing-level chemicals, and one day said, “You know what, we can make steroids in here if we want”. These chemical companies are not licensed to produce drugs, and do not have to comply with even the minimal of GMP guidelines. They are not inspected. Rarely do they have the capacity to produce very pure products. Still, they very often do produce drugs. In fact, it is estimated that HALF of all drugs sold in China come from this illegal chemical market. This number is significantly higher with anabolic steroids.

It doesn’t matter how much you filter a solution. Many things can pass through a .22-micro screen. If you are making drugs with impure steroid APIs, you will produce underground steroids that are impure.

While I concede that there are many underground products of acceptable (safe) purity, the market at its core is completely unregulated, and feeds off a completely unregulated supply chain of rouge chemical companies.

So, in short, it is my opinion now, as it as been for a very long time, that consumers:

SHOULD NOT KNOWINGLY USE UNDERGROUND ANABOLIC STEROIDS

Introduction to Atropin HGH

Atropin Human Growth Hormone (GH) is a peptide hormone. It stimulates growth and cell reproduction in humans. It is developed through Protein Secretion Technology and is 191 Amino Acid. Single chain polypeptide hormone that is synthesized, stored, and secreted by the somatotroph cells within the lateral wings of the anterior pituitary gland. Somatotrophin refers to the growth hormone produced natively in animals, whereas the term somatropin refers to growth hormone produced by recombinant DNA technology, and is abbreviated “rhGH” in humans.

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Growth hormone is used clinically to treat children’s growth disorders and adult growth hormone deficiency. In recent years, replacement therapies with human growth hormones (HGH) have become popular in the battle against aging. Reported effects of Atropin HGH include decreased body fat, increased muscle mass, increased bone density, increased energy levels, improved skin tone and texture, and improved immune system function. At this time Atropin HGH is still considered a very complex hormone and many of its functions are still unknown.

In its role as an anabolic agent, HGH has been used by competitors in sports since the 1970s, and it has been banned by the IOC and NCAA. Traditional urine analysis could not detect doping with HGH, so the ban was unenforceable until the early 2000s, when blood tests that could distinguish between natural and artificial HGH were developed.

Blood tests conducted by WADA at the 2004 Olympic Games in Athens, Greece primarily targeted HGH.

Common Uses of Atropin Human Growth Hormone

• Growth Hormone Deficiency
• Treatment for SGA and IUGR
• Idiopathic Short Stature
• AIDS Wasting and Cachexia
• Short Stature Caused by Turner’s Syndrome
• Short Stature Caused by Prader-Willi Syndrome
• Growth Problems Caused by Short Bowel Syndrome
• Improper Growth in Children with Renal Disease
• Body Building Enhancement Drug
• Weight Loss Drug
• Anti-Aging Drug
• Treatment for Children with Rheumatoid Arthritis
• Osteoporosis Treatment
• Treatment for Children with XLH

Side Effects to Atropin HGH

Hypoglycemia
Hypoglycemia is the opposite of diabetes. In people with diabetes, their bodies do not produce an adequate amount of insulin, leading to dangerously high glucose levels. People with hypoglycemia have too much insulin, leading to too low glucose levels. Because HGH increases the level of insulin in your body, some people have suffered from hypoglycemia after enduring HGH therapy.

Acromeglia
Acromeglia is a disease that causes abnormal bone growth. HGH cannot cause acromeglia, but it can speed up the progression of the disease in people predisposed to it.

Extended Belly
When used as a bodybuilding therapy, HGH can cause a bodybuilder to have an extended belly if the drug is not used as directed. However, this defect is rare in users who administor HGH properly.

Carpal Tunnel Syndrome
Carpal tunnel is caused by a pinched nerve in the wrist. It can lead to loss of hand movement. Atropin HGH has been known to cause carpal tunnel in users who do not administor HGH properly.

Joint Pain
Because of its ability to cause growth in a persons body, some users report joint pain while taking HGH. This side effect is usually temporary.

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Operation Roid Runner bust update ( UGL appears to be Pro Lab)

VIDEO OF STEROIDS BUST!

Corbett announced the arrests of the following people at a news conference this morning in Lemoyne, Pa.:

* Christopher Niemczyk, 31, 1013 Old Course Lane, Williams Township, is charged with four counts of delivery of steroids, one count of possession with intent to deliver steroids, one count of possession with intent to deliver ecstasy, one count of possession of drug paraphernalia, one count of misbranding Ketamine and one count of criminal conspiracy.
* Marcus Lazaro, 29, 123 Somerset St., Freemansburg, is charged with three counts of delivery of steroids, two counts of possession with intent to deliver steroids, two counts of criminal conspiracy, two counts of dealing in the proceeds of an unlawful activity, one count of manufacturing steroids and one count of possession of drug paraphernalia.
* John Sassaman, 51, 1803 Stratford Court, Salisbury Township, is charged with four counts of delivery of steroids and one count of criminal conspiracy.
* Chad Gillespie, 33, 740 Fourth St., Catasauqua, is charged with two counts of criminal conspiracy, one count of possession with intent to deliver steroids, one count of manufacturing steroids and one count of dealing in proceeds of an unlawful activity.
* George Koufalis, 34, 2158 Woodridge Drive, Lower Macungie Township, is charged with two counts of delivery of steroids, one count of possession with intent to deliver steroids, one count of possession of drug paraphernalia and one count of criminal conspiracy.
* Robert Greynolds, 28, of Middletown, Pa., is charged with nine counts of delivery of steroids, one count of possession of drug paraphernalia, one count of carrying a firearm without a license, one count of criminal conspiracy and one count of criminal use of a communication facility.
* Joel France, 42, of Harrisburg, is charged with three counts of delivery of steroids, one count of criminal conspiracy and one count of criminal use of a communication facility.
* Christopher Levan, 36, of Mechanicsburg, Pa., is charged with one count of delivery of steroids and one count of criminal conspiracy.
* Stacy Garonzik, 38, of Shiremanstown, Pa., is charged with one count of delivery of steroids, one count of possession with intent to deliver steroids, one count of dealing in proceeds of unlawful activity and one count of criminal conspiracy.
* Eric Garonzik, 39, of Mechanicsburg, Pa., is charged with one count of delivery of steroids, one count of possession with intent to deliver steroids, one count of dealing in proceeds of unlawful activity and one count of criminal conspiracy.

“Like any illegal drug, steroids come with negative and dangerous physical effects,” Corbett says in a news release. “We need to do everything we can to make sure that the public, especially young men, are aware of the dangers of using steroids, and we need to take those who distribute this poison off our streets.”

Corbett said the Garonziks injected clients with steroids in the office of their gym, Kinetics, which is now closed. Corbett said many of the steroid deliveries in the Harrisburg area took place near Gold’s Gym in Swatara Township.

He said the Garonziks, Lazaro and Gillespie obtained steroids by placing Internet orders to people in China and Mexico and paying for the via wire transfer. A grand jury investigation determined $170,000 was sent overseas between January 2004 and this year. The senders allegedly used fictitious names and structured the wire payments so they would always be less than $1,000.

Lazaro researched how to turn powder steroids into those that could be injected, and he and Gillespie started manufacturing the drugs at Lazaro’s home and branded them “Pro Lab,” Corbett says. Sassaman and Koufalis, both bodybuilders, allegedly obtained “Pro Lab” steroids from Lazaro and Gillespie and sold them to others to pay for the expense of bodybuilding competitions.

When officials searched Lazaro’s home, they allegedly seized more than nine pounds of bulk steroids, numerous syringes, a 9mm firearm and various items, such as filters, oils and alcohols used to manufacture steroids. During the course of the entire investigation, agents seized more than 700 bottles of steroids, 1,337 pills containing steroids, nine pounds of bulk steroids, $28,000 and four other firearms. The investigation is ongoing.

ps:please post this link of this video to your friends who use steroids!

Underground Steroid Labs, UGL